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Gas Chromatography of 17-Ketosteroid Oximes. Formation of Nitriles by Beckmann Fission

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Oxime derivatives (methoxime, benzyloxime, trimethylsilyloxime) of 17-ketosteroids will, under some gas chromatographic conditions, undergo Beckmann fission in the injector zone. The result of this effect is partial or total conversion of the steroid derivative to a nitrile.



出版机构:Taylor & Francis刊物名称:Analytical Letters
出版时间:1971
ISSN:0003-2719
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